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阴香叶片精油中右旋龙脑含量近红外预测模型构建研究
李兵1, 伍观娣1, 连辉明1, 林涛2, 姚燕飞3, 李毅4, 詹金婵4, 何波祥1
1.广东省林业科学研究院;2.平远县林业科学研究所;3.广东华清园生物科技有限公司;4.广东森霖造绿有限公司
摘要:
为建立阴香 Cinnamomum burmannii 叶片中精油右旋龙脑含量的近红外光谱预测模型,使用 波通(PERTEN)公司的 DA7250 近红外光谱分析仪,在 950~1 650 nm 的光谱范围内,分析了 76 个阴香 叶片样本的光谱数据,经过光谱预处理,并比较选择最佳预处理方法、最佳光谱波段范围和最佳主成分 数,采用偏最小二乘法(PLS)建立阴香叶片精油中右旋龙脑含量近红外光谱模型。结果表明:采用一 阶导数 - 标准正态变量转换法(FD-SNV)对光谱进行预处理且当最佳主成分数为 16 时,得到最优模型, 其校正集均方根误差(RMSEC)为 7.407 1,校正集相关系数(RC)为 0.931 4,交互验证集均方根误差 (RMSEV)为 13.482 2,交互验证集相关系数(RV)为 0.775 9。说明预测值与测量值具有显著的相关性, 该预测模型具有一定的准确性,可以用于阴香叶片精油中右旋龙脑含量进行快速预测。
关键词:  阴香  右旋龙脑含量  近红外光谱技术  预测模型
DOI:
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基金项目:广东省林业科技创新项目(2020KJCX001,2022KJCX006,2018KJCX034)
Establishment of A Near-infrared Prediction Model for the D-borneol Content in the Essential Oil from Leaves of Cinnamomum burmannii
libing1, WU Guandi1, LIAN Huiming1, LIN Tao2, YAO Yanfei3, LI Yi4, ZHAN Jinchan4, HE Boxiang1
1.Guangdong Academy of Forestry;2.Pingyuan Research Institute of Forestry;3.Guangdong Huaqingyuan Biotechnology Co., Ltd;4.Guangdong Senlin Greening Co.,Ltd
Abstract:
In order to establishment of a near infrared detection model for D-borneol content in the essential oil for leaves of Cinnamomum burmannii, the spectral data of 76 leaves of C. burmannii by the DA7250 Near Infrared Spectrum Analyzer of PERTEN, Co. Ltd, in the spectral of 950 nm to 1 650 nm, establishment on a near infrared detection model for D-borneol content in essential oil from leaves of C.burmannii by the PLS, after spectral preprocessing, compare and choose the best of preprocessing method, spectral band range and principal component.In a result, you can get the optimal model after preprocess the spectrum by the FD-SNV and when the principal component is 16, RC is 0.931 4, RMSEC is 7.407 1, RV is 0.775 9, RMSEV is 13.482 2. It directions that the predicted value has a significant correlation with the measured value, and the model has a certain prediction accuracy, it can help us to predict the D-borneol content in essential oil from leaves of C. burmannii faster.
Key words:  Cinnamomum burmannii  D-borneol  NIR  prediction model